{"id":981,"date":"2019-09-24T11:19:18","date_gmt":"2019-09-24T11:19:18","guid":{"rendered":"https:\/\/ilkercivil.com\/staging\/?p=981"},"modified":"2020-02-24T11:12:37","modified_gmt":"2020-02-24T11:12:37","slug":"voc","status":"publish","type":"post","link":"https:\/\/ilkercivil.com\/staging\/2019\/09\/24\/voc\/","title":{"rendered":"Ki\u015fisel U\u00e7ucu Organik Bile\u015fiklerin(VOC)\u00d6l\u00e7\u00fclmesi"},"content":{"rendered":"

VOC normal oda s\u0131cakl\u0131\u011f\u0131nda y\u00fcksek buhar bas\u0131nc\u0131na sahip organik bile\u015fiklere u\u00e7ucu organik bile\u015fikler denir. Y\u00fcksek buhar bas\u0131nc\u0131 d\u00fc\u015f\u00fck bir kaynama noktas\u0131ndan kaynaklanmaktad\u0131r.  U\u00e7ucu organik bile\u015fikler say\u0131s\u0131z, \u00e7e\u015fitli ve her yerde bulunur.<\/p>\n

U\u00e7ucu organik bile\u015fikler de\u011fi\u015fik y\u00f6ntemlerle tayin edilebilir, bunlar ;<\/p>\n

    \n
  1. Foto \u0130yonizasyon Dedekt\u00f6r\u00fc (PID)<\/li>\n
  2. Alev \u0130yonizasyon Dedekt\u00f6r\u00fc (FID)<\/li>\n
  3. Kolorimetrik \u00f6rnekleme t\u00fcpleri<\/li>\n
  4. Elektrokimyasal Sens\u00f6rl\u00fc cihazlar<\/li>\n<\/ol>\n

    En do\u011fru ve ayr\u0131nt\u0131l\u0131 sonucu sahada \u00f6rnekleme t\u00fcpleri kullan\u0131larak al\u0131nan numunenin FID dedekt\u00f6r\u00fc olan enstr\u00fcmantal bir cihaz ile analizinin yap\u0131lmas\u0131d\u0131r. Bu yaz\u0131da TS ISO 16200-1 standard\u0131 ile ki\u015fisel VOC \u00f6l\u00e7\u00fcm\u00fcn\u00fcn sahada \u00f6rneklenmesi, analizinin yap\u0131lmas\u0131 ve raporlanmas\u0131 hakk\u0131nda bilgilerden bahsedilecektir.<\/p>\n

    \u00d6l\u00e7\u00fcmlerin Yap\u0131lmas\u0131<\/strong><\/h2>\n

    Sahada VOC \u00f6rneklemesi i\u00e7in EN 1232 standard\u0131 gereklilikleri sa\u011flayan 0-200 cc\/dk ile \u00f6rnekleme yapabilen bir pompa, TS ISO 16200-1 standard\u0131na uygun \u00f6rnekleme t\u00fcpleri, birincil standart hava ak\u0131\u015f kalibrat\u00f6r\u00fcne ihtiya\u00e7 vard\u0131r. Sahada kullan\u0131lacak pompa \u00f6l\u00e7\u00fcme ba\u015flamadan \u00f6nce \u00f6l\u00e7\u00fcm d\u00fczene\u011fi kurularak hava ak\u0131\u015f kalibrat\u00f6r\u00fc ile do\u011frulanmas\u0131 gerekmektedir. Ayn\u0131 do\u011frulama i\u015flemi \u00f6rnekleme sonunda da yap\u0131lmal\u0131d\u0131r. Ba\u015flama ve biti\u015f ak\u0131\u015f h\u0131zlar\u0131 aras\u0131ndaki fark %10\u2019nu ge\u00e7memelidir. E\u011fer bu fark %10\u2019dan b\u00fcy\u00fckse numune at\u0131lmal\u0131 ve \u00f6rnekleme tekrar edilmelidir.<\/p>\n

    \u00d6rnekleme t\u00fcp\u00fcn\u00fcn her iki ucu da k\u0131r\u0131larak bir t\u00fcp tutucuya yerle\u015ftirilir. Bir hortum yard\u0131m\u0131yla \u00f6rnekleme pompas\u0131na ba\u011flant\u0131s\u0131 yap\u0131l\u0131r. Burada dikkat edilmesi gereken en \u00f6nemli husus t\u00fcp\u00fcn y\u00f6n\u00fcd\u00fcr. \u00d6rnekleme t\u00fcpleri ana ve emniyet olmak \u00fczere iki k\u0131s\u0131mdan olu\u015fmaktad\u0131r. D\u0131\u015far\u0131dan \u00f6rneklenecek havan\u0131n \u00f6nce ana k\u0131s\u0131mdan daha sonra emniyet k\u0131sm\u0131ndan ge\u00e7ecek \u015fekilde t\u00fcp tutucuya yerle\u015ftirilmesi gerekmektedir.<\/p>\n

    \"VOC      \"VOC<\/p>\n

    \u00d6rnekleme t\u00fcp\u00fc solunum hizas\u0131na gelecek \u015fekilde personelin \u00fczerine \u015fekildeki gibi tak\u0131l\u0131r.Gerekli ba\u011flant\u0131lar yap\u0131ld\u0131ktan sonra pompa \u00e7al\u0131\u015ft\u0131r\u0131l\u0131r ve uygun \u00f6rnekleme s\u00fcresinde \u00f6rnekleme yap\u0131l\u0131r. Bu s\u00fcrenin belirlenmesinde iki \u00f6nemli husus bulunmaktad\u0131r. Bunlardan ilki TS ISO 16200-1 standard\u0131n\u0131n gerekliklerini sa\u011flamak i\u00e7in en az 10 litre hacimde numune al\u0131nmas\u0131, ikincisi ise TS EN 689 standard\u0131nda belirtilen \u00f6rnekleme s\u00fcrelerine uyulmas\u0131d\u0131r.<\/p>\n

    \u00d6rnekleme tamamland\u0131\u011f\u0131nda, \u00f6rnekleme t\u00fcp\u00fc d\u00fczenekten ayr\u0131l\u0131r ve t\u00fcp\u00fcn her iki ucu da kapaklarla kapat\u0131l\u0131r. T\u00fcpler ayr\u0131 ayr\u0131 i\u015faretlenmelidir. Bu i\u015faretlemede \u00e7\u00f6z\u00fcc\u00fc ihtiva eden boyal\u0131 kalemler veya yap\u0131\u015fkan etiketler t\u00fcplerin i\u015faretlenmesinde kullan\u0131lmamal\u0131d\u0131r.<\/p>\n

    Sahada al\u0131nmas\u0131 gereken k\u00f6r numune, numune alma i\u00e7in kullan\u0131lan t\u00fcpler ile \u00f6zde\u015f t\u00fcpler(ayn\u0131 LOT numaras\u0131na sahip) kullan\u0131larak haz\u0131rlanmal\u0131d\u0131r. Numuneler 8 saat i\u00e7inde analiz edilmeyecekse, temiz, kaplamas\u0131z ve s\u0131zd\u0131rmaz metal veya cam kaplar i\u00e7inde muhafaza edilmelidir.  \u00d6rneklenen maddelerin u\u00e7uculuklar\u0131na ba\u011fl\u0131 olarak kuru buz veya derin dondurucu i\u00e7erisinde muhafaza edilmelidir. Daha az u\u00e7ucu  maddeler 5o<\/sup>C\u2019nin alt\u0131nda muhafaza edilmelidir.<\/p>\n

    \u00d6rneklenen numuneler m\u00fcmk\u00fcn oldu\u011funca h\u0131zl\u0131 analiz edilmelidir. \u00d6rnekleme t\u00fcp\u00fcndeki aktif karbona adsorbe olan VOC\u2019ler standarda belirtilen uygun desorpsiyon \u00e7\u00f6z\u00fcc\u00fcs\u00fc ile \u00e7\u00f6z\u00fcl\u00fcr ve gaz kromatografi cihaz\u0131nda analiz edilir.<\/p>\n

    VOC Konsantrasyonun Hesaplanm<\/strong>as\u0131<\/strong><\/h2>\n

    Numunesi al\u0131nm\u0131\u015f maddenin k\u00fctlesel deri\u015fimi, miligram\/metrek\u00fcp olarak, a\u015fa\u011f\u0131daki e\u015fitlik yard\u0131m\u0131yla hesaplan\u0131r:<\/p>\n

    \"\"<\/p>\n

    cm<\/sub>: Numunesi al\u0131nm\u0131\u015f havadaki deneye t\u00e2bi tutulan maddenin deri\u015fimi, mg\/mL,<\/p>\n

    Dm<\/sub>: mf<\/sub>\u2019ye kar\u015f\u0131l\u0131k gelen numune t\u00fcp\u00fc y\u00fckleme seviyesinde desorpsiyon verimi,<\/p>\n

    mF<\/sub>: Ger\u00e7ek numunede (t\u00fcp\u00fcn \u00f6n b\u00f6l\u00fcm\u00fcnde) deneye t\u00e2bi tutulan havadaki UOB\u2019nin k\u00fctlesi, mg<\/p>\n

    mR<\/sub>: Ger\u00e7ek numunede (t\u00fcp\u00fcn geri veya arka b\u00f6l\u00fcm\u00fcnde) deneye t\u00e2bi tutulan havadaki UOB\u2019nin k\u00fctlesi, mg<\/p>\n

    mB<\/sub>: K\u00f6r numune t\u00fcp\u00fcndeki mevcut deneye t\u00e2bi tutulan madde k\u00fctlesi,mg<\/p>\n

    V: Al\u0131nan numune hacmi, L dir.<\/p>\n

    Not – Deri\u015fimin belirtilen \u015fartlara d\u00fczeltilerek ifade edilmesi istenildi\u011finde, \u00f6rne\u011fin 25 \u00b0C\u2019da ve 101 kPa\u2019da, e\u015fitlik a\u015fa\u011f\u0131daki gibi olur:<\/p>\n

    \"\"<\/p>\n

    Burada;<\/p>\n

    Cc: Belirtilen \u015fartlara d\u00fczeltilmi\u015f al\u0131nan hava numunesindeki deneye t\u00e2bi tutulan madde deri\u015fimi; mg\/mL<\/p>\n

    P: Numunesi al\u0131nan havan\u0131n ger\u00e7ek bas\u0131n\u00e7\u0131, kilopaskal<\/p>\n

    T: Numunesi al\u0131nan havan\u0131n ger\u00e7ek s\u0131cakl\u0131\u011f\u0131, derece Celsiusdur.<\/p>\n

    Deneye t\u00e2bi tutulan maddenin havadaki hacim kesri, metre k\u00fcpte mililitre olarak, a\u015fa\u011f\u0131daki e\u015fitlik ile hesaplan\u0131r.<\/p>\n

    \"\"<\/p>\n

    Burada;<\/p>\n

    Cv<\/sub>: Deneye t\u00e2bi tutulan maddenin havadaki hacim kesri, mL\/m3<\/p>\n

    M: Deneye t\u00e2bi tutulan ilgili maddenin mol k\u00fctlesi, gram\/mol<\/p>\n

    24,5: 25 \u00b0C\u2019da ve 101 kPa\u2018da mol hacmidir.<\/p>\n

    TS EN 689 Kimyasal Maddelerin Solunmas\u0131yla Maruziyetin \u00d6l\u00e7\u00fclmesi<\/a><\/p>\n

    K\u0130MYASAL MADDELERLE \u00c7ALI\u015eMALARDA SA\u011eLIK VE G\u00dcVENL\u0130K \u00d6NLEMLER\u0130 HAKKINDA Y\u00d6NETMEL\u0130K<\/a><\/p>\n\n","protected":false},"excerpt":{"rendered":"

    VOC normal oda s\u0131cakl\u0131\u011f\u0131nda y\u00fcksek buhar bas\u0131nc\u0131na sahip organik bile\u015fiklere u\u00e7ucu organik bile\u015fikler denir. Y\u00fcksek buhar bas\u0131nc\u0131 d\u00fc\u015f\u00fck bir kaynama […]<\/p>\n","protected":false},"author":1,"featured_media":988,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_uag_custom_page_level_css":"","site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"default","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","ast-disable-related-posts":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"_jetpack_memberships_contains_paid_content":false,"footnotes":""},"categories":[47],"tags":[49,50],"class_list":["post-981","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-is-hijyeni","tag-kisisel-voc-olcumu","tag-maruziyet"],"yoast_head":"\nVOC Ki\u015fisel U\u00e7ucu Organik Bile\u015fikler - 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